Table 3 Methodology for choosing a reagent for the development of the spectrophotometric methods for the determination of dihydropyridines CCBs
Analyte | Reagent | Optimal conditions (wavelenght, solvent, molar concentration) | Possibility of application | Remark |
|---|---|---|---|---|
AML | BCG | 415 nm, MetOH, 5.0*10–4 M | No | pH adjustment |
BTB | 405 nm, MetOH, 2.49*10–4 M | No | pH adjustment | |
BPB | 598 nm, MetOH, 6.0*10–5 M | Yes | Methanol medium, absorption maximum at a wavelength 598 nm | |
BCP | 415 nm, EtAc, 2.26*10–4 M | No | pH adjustment | |
CR | 398 nm, AcN, 2.5*10–4 M | No | pH adjustment | |
PR | 350 nm, AcN, 1.0*10–4 M | No | No interaction | |
TB | 405 nm, AcN, 1.0*10–4 M | No | pH adjustment | |
NIF | BCG | 405 nm, MetOH, 5.0*10–4 M | No | pH adjustment |
BTB | 398 nm, MetOH, 2.76*10–4 M | No | pH adjustment | |
BPB | 598 nm, MetOH, 5.0*10–4 M | Yes | Methanol medium, absorption maximum at a wavelength 598 nm | |
BCP | 415 nm, EtAc, 2.26*10–4 M | No | pH adjustment | |
CR | 380 nm, AcN, 2.5*10–4 M | No | pH adjustment | |
PR | 350 nm, AcN, 2.26*10–4 M | No | No interaction | |
NIT | BCG | 415 nm, MetOH, 5.0*10–4 M | No | pH adjustment |
BTB | 350 nm, MetOH, 2.77*10–5 M | No | pH adjustment | |
BPB | 598 nm, metOH, 5,0*10–4 M | Yes | Methanol medium, absorption maximum at a wavelength 598 nm | |
BCP | 415 nm, EtAc, 2.26*10–4 M | No | No interaction | |
CR | 398 nm, AcN, 2.5*10–4 M | No | pH adjustment | |
TB | 350 nm, AcN, 1.0*10–4 M | No | No interaction | |
NIM | BTB | 423 nm, MetOH, 5.0*10–5 M | No | pH adjustment |
BPB | 598Â nm, AcN | Yes | Acetonitrile medium, absorption maximum at a wavelength 598Â nm | |
BCP | 420 nm, MetOH, 5.0*10–5 M | No | pH adjustment | |
CR | 423 nm, EtOH, 1.0*10–4 M | No | pH adjustment | |
TB | 390 nm, AcN, 1.0*10–4 M | No | pH adjustment | |
LAC | BCG | MetOH, 1*10–3 M | No | No interaction |
BTB | MetOH, 1.0*10–3 M | No | No interaction | |
BPB | AcN, 1.0*10–3 M | Yes | Acetonitrile medium, absorption maximum at a wavelength 598 nm | |
BCP | MetOH, 1.0*10–3 M | No | No interaction | |
MR | AcN, 1.0*10–3 M | No | No interaction | |
CR | MetOH, 1.0*10–3 M | No | No interaction | |
PR | MetOH, 1.0*10–3 M | No | No interaction | |
TB | MetOH, 1.0*10–3 M | No | No interaction | |
LAML | BCG | MetOH, 1.0*10–3 M | No | No interaction |
BTB | MetOH, 1.0*10–3 M | No | No interaction | |
BPB | MetOH, 1.0*10–3 M | Yes | Methanol medium, absorption maximum at a wavelength 598 nm | |
BCP | MetOH, 1.0*10–3 M | No | No interaction | |
MR | AcN, 1.0*10–3 M | No | No interaction | |
CR | MetOH, 1.0*10–3 M | No | No interaction | |
PR | MetOH, 1.0*10–3 M | No | No interaction | |
TB | MetOH, 1.0*10–3 M | No | No interaction |