Figure 6

(a) 2D 3QMAS spectra of solvated Alq 3 after the removal of ethanol. Optimised excitation and conversion pulse lengths were 3.8 μs and 1.8 μs. A total of 60 t1 increments was taken with 5 μs of dwell time with 576 transients per increment. The recycling dealy was 1s. Total experiment time was 9 hours 42 mins. (b) The anisotropic slice along the direction parallel to the F2 dimension. (c) The isotropic projection along the F1 dimension.